Structures published

Decacarbonyl(μ-ethylidenimino-1κN:2κC)-μ-hydrido-triangulo-triosmium(3 Os—–Os)

C₁₂H₅NO₁₀Os₃

Powell, Cynthia B.Powell, Gregory L.Archambeau, Ashley K.Wilson, Kylie M.

IUCrData (2019) 4, 10 x191386

a=9.56470(6)Å b=11.59555(8)Å c=15.61610(11)Å

α=90° β=90° γ=90°

Μ-Acetato-1κO:2κO-μ-propanoato-1κO:2κO'-bis[tris(4-methylphenyl)phosphane]-1κP,2κP'-bis(dicarbonylosmium)(Os—–-Os) dichloromethane monosolvate

C₅₁H₅₀O₈Os₂P_2,CH₂Cl₂

Wilson, Kylie M.Swartout, John W.Touchton, Henry A.Lambert, Erica N.Johnstone, James E.Archambeau, Ashley K.Marolf, David M.Mikeska, Emily R.Lynch, Vincent M.Nesterov, Vladimir N.Reinheimer, Eric W.Powell, Gregory L.Powell, Cynthia B.

Acta Crystallographica Section C (2019) 75, 5 529-537

a=18.5007(4)Å b=18.5396(4)Å c=14.8090(3)Å

α=90° β=91.9976(17)° γ=90°

Bis(μ-acetato-1κO:2κO)bis(tricarbonylosmium)(Os—–-Os)

C₁₀H₆O₁₀Os₂

Wilson, Kylie M.Swartout, John W.Touchton, Henry A.Lambert, Erica N.Johnstone, James E.Archambeau, Ashley K.Marolf, David M.Mikeska, Emily R.Lynch, Vincent M.Nesterov, Vladimir N.Reinheimer, Eric W.Powell, Gregory L.Powell, Cynthia B.

Acta Crystallographica Section C (2019) 75, 5 529-537

a=7.6949(5)Å b=14.3612(10)Å c=13.8623(9)Å

α=90° β=105.2020(10)° γ=90°

Bis(μ-propanoato-1κO:2κO)bis(tricarbonylosmium)(Os—–-Os)

C₁₂H₁₀O₁₀Os₂

Wilson, Kylie M.Swartout, John W.Touchton, Henry A.Lambert, Erica N.Johnstone, James E.Archambeau, Ashley K.Marolf, David M.Mikeska, Emily R.Lynch, Vincent M.Nesterov, Vladimir N.Reinheimer, Eric W.Powell, Gregory L.Powell, Cynthia B.

Acta Crystallographica Section C (2019) 75, 5 529-537

a=9.79942(10)Å b=15.51827(19)Å c=21.7339(2)Å

α=90° β=90° γ=90°

Pentacarbonyl-1κ^2^C,2κ^3^C-bis(μ-propanoato-1κO:2κO)[tris(4-methylphenyl)phosphane-1κP]diosmium(Os—–-Os)

C₃₂H₃₁O₉Os₂P

Wilson, Kylie M.Swartout, John W.Touchton, Henry A.Lambert, Erica N.Johnstone, James E.Archambeau, Ashley K.Marolf, David M.Mikeska, Emily R.Lynch, Vincent M.Nesterov, Vladimir N.Reinheimer, Eric W.Powell, Gregory L.Powell, Cynthia B.

Acta Crystallographica Section C (2019) 75, 5 529-537

a=10.0952(2)Å b=11.6630(3)Å c=13.7536(3)Å

α=88.6185(19)° β=86.7627(18)° γ=86.9563(19)°

Bis(μ-acetato-1κO:2κO)pentacarbonyl-1κ^2^C,2κ^3^C-[tris(4-methylphenyl)phosphane-1κP]diosmium(Os—–-Os)

C₃₀H₂₇O₉Os₂P

Wilson, Kylie M.Swartout, John W.Touchton, Henry A.Lambert, Erica N.Johnstone, James E.Archambeau, Ashley K.Marolf, David M.Mikeska, Emily R.Lynch, Vincent M.Nesterov, Vladimir N.Reinheimer, Eric W.Powell, Gregory L.Powell, Cynthia B.

Acta Crystallographica Section C (2019) 75, 5 529-537

a=10.452(4)Å b=11.229(4)Å c=13.045(5)Å

α=82.813(6)° β=89.157(8)° γ=89.457(9)°

Bis(μ-formato-1κO:2κO)bis[tris(4-methylphenyl)phosphane]-1κP,2κP-bis(dicarbonylosmium)(Os—–-Os)

C₄₈H₄₄O₈Os₂P₂

Wilson, Kylie M.Swartout, John W.Touchton, Henry A.Lambert, Erica N.Johnstone, James E.Archambeau, Ashley K.Marolf, David M.Mikeska, Emily R.Lynch, Vincent M.Nesterov, Vladimir N.Reinheimer, Eric W.Powell, Gregory L.Powell, Cynthia B.

Acta Crystallographica Section C (2019) 75, 5 529-537

a=10.7707(4)Å b=10.8014(4)Å c=20.3790(7)Å

α=104.3930(10)° β=91.0090(10)° γ=98.9930(10)°

Bis(μ-propanoato-1κO:2κO)bis[tris(4-methylphenyl)phosphane]-1κP,2κP-bis(dicarbonylosmium)(Os—–-Os), dichloromethane monosolvate

C₅₂H₅₂O₈Os₂P_2,CH₂Cl₂

Wilson, Kylie M.Swartout, John W.Touchton, Henry A.Lambert, Erica N.Johnstone, James E.Archambeau, Ashley K.Marolf, David M.Mikeska, Emily R.Lynch, Vincent M.Nesterov, Vladimir N.Reinheimer, Eric W.Powell, Gregory L.Powell, Cynthia B.

Acta Crystallographica Section C (2019) 75, 5 529-537

a=18.4968(6)Å b=18.7369(7)Å c=14.9214(6)Å

α=90° β=91.806(2)° γ=90°

Bis(μ-acetato-1κO:2κO)bis[tris(4-methylphenyl)phosphane]-1κP,2κP-bis(dicarbonylosmium)(Os—–-Os) p-xylene sesquisolvate

C₅₀H₄₈O₈Os₂P_2,1.5(C₈H₁₀)

Wilson, Kylie M.Swartout, John W.Touchton, Henry A.Lambert, Erica N.Johnstone, James E.Archambeau, Ashley K.Marolf, David M.Mikeska, Emily R.Lynch, Vincent M.Nesterov, Vladimir N.Reinheimer, Eric W.Powell, Gregory L.Powell, Cynthia B.

Acta Crystallographica Section C (2019) 75, 5 529-537

a=12.81225(16)Å b=14.8455(2)Å c=16.6818(2)Å

α=98.1785(11)° β=101.7904(11)° γ=113.3846(14)°

Structures by: Wilson K. M.

Total: 9

Decacarbonyl(μ-ethylidenimino-1κ<i>N</i>:2κ<i>C</i>)-μ-hydrido-<i>triangulo</i>-triosmium(3 <i>Os</i>—–<i>Os</i>)

Μ-Acetato-1κ<i>O</i>:2κ<i>O</i>-μ-propanoato-1κ<i>O</i>:2κ<i>O</i>'-bis[tris(4-methylphenyl)phosphane]-1κ<i>P</i>,2κ<i>P</i>'-bis(dicarbonylosmium)(<i>Os</i>—–-<i>Os</i>) dichloromethane monosolvate

Bis(μ-acetato-1κ<i>O</i>:2κ<i>O</i>)bis(tricarbonylosmium)(<i>Os</i>—–-<i>Os</i>)

Bis(μ-propanoato-1κ<i>O</i>:2κ<i>O</i>)bis(tricarbonylosmium)(<i>Os</i>—–-<i>Os</i>)

Pentacarbonyl-1κ^2^<i>C</i>,2κ^3^<i>C</i>-bis(μ-propanoato-1κ<i>O</i>:2κ<i>O</i>)[tris(4-methylphenyl)phosphane-1κ<i>P</i>]diosmium(<i>Os</i>—–-<i>Os</i>)

Bis(μ-acetato-1κ<i>O</i>:2κ<i>O</i>)pentacarbonyl-1κ^2^<i>C</i>,2κ^3^<i>C</i>-[tris(4-methylphenyl)phosphane-1κ<i>P</i>]diosmium(<i>Os</i>—–-<i>Os</i>)

Bis(μ-formato-1κ<i>O</i>:2κ<i>O</i>)bis[tris(4-methylphenyl)phosphane]-1κ<i>P</i>,2κ<i>P</i>-bis(dicarbonylosmium)(<i>Os</i>—–-<i>Os</i>)

Bis(μ-propanoato-1κ<i>O</i>:2κ<i>O</i>)bis[tris(4-methylphenyl)phosphane]-1κ<i>P</i>,2κ<i>P</i>-bis(dicarbonylosmium)(<i>Os</i>—–-<i>Os</i>), dichloromethane monosolvate

Bis(μ-acetato-1κ<i>O</i>:2κ<i>O</i>)bis[tris(4-methylphenyl)phosphane]-1κ<i>P</i>,2κ<i>P</i>-bis(dicarbonylosmium)(<i>Os</i>—–-<i>Os</i>) <i>p</i>-xylene sesquisolvate